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Full Description

1.1 These test methods cover procedures for the chemical, mass spectrometric, and spectrochemical analysis of nuclear-grade boron carbide powder and pellets to determine compliance with specifications.

1.2 The analytical procedures appear in the following order:

Sections
Total Carbon by Combustion and Gravimetry7-17
Total Boron by Titrimetry18-28
Isotopic Composition by Mass Spectrometry29-38
Chloride and Fluoride Separation by Pyrohydrolysis39-45
Chloride by Constant-Current Coulometry46-54
Fluoride by Ion-Selective Electrode55-63
Water by Constant-Voltage Coulometry64-72
Impurities by Spectrochemical Analysis73-81
Soluble Boron by Titrimetry82-95
Soluble Carbon by a Manometric Measurement96-105
Metallic Impurities by a Direct Reader Spectrometric Method106-114
 

Document History

  1. ASTM C791-19


    Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Boron Carbide

    • Most Recent
  2. ASTM C791-12


    Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Boron Carbide

    • Historical Version
  3. ASTM C791-11


    Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Boron Carbide

    • Historical Version
  4. ASTM C791-04

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    Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Boron Carbide

    • Historical Version
  5. ASTM C791-83(2000)


    Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Boron Carbide

    • Historical Version