Published annually in October.

This volume contains 89 standards.

Volume 03.06 covers molecular spectroscopy, and includes standards pertaining to chromatography, fiberoptics and waveguides, infrared spectroscopy, molecular luminescence, and ultra-violet and visible spectroscopy. It also includes procedures for surface analysis and examines auger electron spectroscopy, x-ray photoelectron spectroscopy, ion beam sputtering, and secondary ion mass spectroscopy (SIMS).