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Full Description

1.1 This practice covers a procedure for the isolation of carbides, borides, TCP (topologically close-packed), and GCP (geometrically close-packed) phases (Note 1) in nickel and nickel-iron base gamma prime strengthened alloys. Contamination of the extracted residue by coarse matrix (gamma) or gamma prime particles, or both, reflects the condition of the alloy rather than the techniques mentioned in this procedure.

1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (See 4.3.2.1 and 5.1.1.)

Note 1: Ni3 Ti (eta phase) has been found to be soluble in the electrolyte for some alloys.

FIG. 1 Schematic Diagram of Extraction Cell

 Schematic Diagram of Extraction Cell Schematic Diagram of Extraction Cell

1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

 

Document History

  1. ASTM E963-95(2017)

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    Standard Practice for Electrolytic Extraction of Phases from Ni and Ni-Fe Base Superalloys Using a Hydrochloric-Methanol Electrolyte (Withdrawn 2018)

    • Most Recent
  2. ASTM E963-95(2010)


    Standard Practice for Electrolytic Extraction of Phases from Ni and Ni-Fe Base Superalloys Using a Hydrochloric-Methanol Electrolyte

    • Historical Version
  3. ASTM E963-95(2004)


    Standard Practice for Electrolytic Extraction of Phases from Ni and Ni-Fe Base Superalloys Using a Hydrochloric-Methanol Electrolyte

    • Historical Version
  4. ASTM E963-95(2000)


    Standard Practice for Electrolytic Extraction of Phases from Ni and Ni-Fe Base Superalloys Using a Hydrochloric-Methanol Electrolyte

    • Historical Version
  5. ASTM E963-95


    Standard Practice for Electrolytic Extraction of Phases from Ni and Ni-Fe Base Superalloys Using a Hydrochloric-Methanol Electrolyte

    • Historical Version