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1.1 These test methods cover two alternative procedures using high-temperature tube furnace combustion methods for the rapid determination of sulfur in samples of coal and coke.

1.2 These test methods appear in the following order:

Sections
Method A - High-Temperature Combustion Method with Acid Base Titration Detection Procedures6-9
Method B - High-Temperature Combustion Method with Infrared Absorption Detection Procedures10-12

Note 1 - High Temperature Combustion Method with Iodimetric Detection procedures, formally Method B in the 2000 version of this standard is still a viable method that may be used.

1.2.1 When automated equipment is used to perform any of the two methods of this test method, the procedures can be classified as instrumental methods. There are several manufacturers that offer to the coal industry equipment with instrumental analysis capabilities for the determination of the sulfur content of coal and coke samples.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See 7.8 and 11.2.

 

Document History

  1. ASTM D4239-17


    Standard Test Method for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion

    • Historical Version
  2. ASTM D4239-18e1


    Standard Test Method for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion

    • Most Recent
  3. ASTM D4239-18


    Standard Test Method for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion

    • Historical Version
  4. ASTM D4239-17


    Standard Test Method for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion

    • Historical Version
  5. ASTM D4239-17


    Standard Test Method for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion

    • Historical Version
  6. ASTM D4239-14e2


    Standard Test Method for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion

    • Historical Version
  7. ASTM D4239-14e1


    Standard Test Method for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion

    • Historical Version
  8. ASTM D4239-14


    Standard Test Method for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion

    • Historical Version
  9. ASTM D4239-13e1


    Standard Test Method for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion

    • Historical Version
  10. ASTM D4239-13


    Standard Test Method for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion

    • Historical Version
  11. ASTM D4239-12


    Standard Test Method for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion

    • Historical Version
  12. ASTM D4239-11


    Standard Test Methods for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion Methods

    • Historical Version
  13. ASTM D4239-10e1


    Standard Test Methods for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion Methods

    • Historical Version
  14. ASTM D4239-10


    Standard Test Methods for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion Methods

    • Historical Version
  15. ASTM D4239-08


    Standard Test Methods for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion Methods

    • Historical Version
  16. ASTM D4239-05

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    Standard Test Methods for Sulfur in the Analysis Sample of Coal and Coke Using High Temperature Tube Furnace Combustion Methods

    • Historical Version
  17. ASTM D4239-04a


    Standard Test Methods for Sulfur in the Analysis Sample of Coal and Coke Using High Temperature Tube Furnace Combustion Methods

    • Historical Version
  18. ASTM D4239-04


    Standard Test Methods for Sulfur in the Analysis Sample of Coal and Coke Using High Temperature Tube Furnace Combustion Methods

    • Historical Version
  19. ASTM D4239-02


    Standard Test Methods for Sulfur in the Analysis Sample of Coal and Coke Using High Temperature Tube Furnace Combustion Methods

    • Historical Version
  20. ASTM D4239-97e1


    Standard Test Methods for Sulfur in the Analysis Sample of Coal and Coke Using High Temperature Tube Furnace Combustion Methods

    • Historical Version